FePcBN-ox

Date

28.03.2023

Synthesis

  1. Mix 59.5 mg of FePcBN-14 sample with 49.7 mg of FePcBN-16-6
  2. Add quartz granules (200 - 400 μm) up to 1.8 ml volume
  3. Place in quartz U-shaped tube
  4. Connect to Quantachrome ChemBET Pulsar system
  5. Turn on gas flow mixture of 28.8 ml/min Ar + 7.2 ml/min O2
  6. Ramp furnace to 350°C at 10 °/min
  7. Hold at 350°C for 240 min
  8. Cool down using fan of the device
  9. Mix with FePcBN-16-2-ox-tg sample

ms = 45.6 mg

Initial sample in U-shaped tube Sample after annealing in oxygen