FePcBN-red

Date

29.03.2023

Synthesis

  1. Mix FePcBN-16-2-OxRed-tg with FePcBN-16-ox-red samples to get 26.5 mg of powder
  2. Add quartz granules (200 - 400 μm) up to 1 ml volume
  3. Place in quartz U-shaped tube
  4. Connect to Quantachrome ChemBET Pulsar system
  5. Turn on 14.26 ml/min H2 gas flow
  6. Ramp furnace to 350°C at 10 °/min
  7. Hold at 350°C for 240 min
  8. Cool down using fan of the device

ms = 6.9 mg