BN Pz6 Vac

Synthesis

Date:

17.02.2023

Protocol:

• Pour boron nitride crucibles with BN Pz6 powder
• Place crucibles into Carbolite tube furnace
• Carefully evacuate tube furnace
• Heat to 1350°C with working vacuum pump and hold for 4 h
• Turn off vacuum pump and let furnace cool down to room temperature

m_{BN Pz6} = 2122 mg

m_{BN Pz6 Vac} = 1285 mg

Notes:

Part of BN Pz6 powder was flown away from crucibles during evacuation.